Photoelectrochemical Water Splitting, 1st Edition

  • Published By:
  • ISBN-10: 1461482984
  • ISBN-13: 9781461482987
  • DDC: 541.35
  • Grade Level Range: College Freshman - College Senior
  • 126 Pages | eBook
  • Original Copyright 2013 | Published/Released May 2014
  • This publication's content originally published in print form: 2013

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This book outlines many of the techniques involved in materials development and characterization for photoelectrochemical (PEC) – for example, proper metrics for describing material performance, how to assemble testing cells and prepare materials for assessment of their properties, and how to perform the experimental measurements needed to achieve reliable results towards better scientific understanding. For each technique, proper procedure, benefits, limitations, and data interpretation are discussed. Consolidating this information in a short, accessible, and easy to read reference guide will allow researchers to more rapidly immerse themselves into PEC research and also better compare their results against those of other researchers to better advance materials development. This book serves as a "how-to" guide for researchers engaged in or interested in engaging in the field of photoelectrochemical (PEC) water splitting. PEC water splitting is a rapidly growing field of research in which the goal is to develop materials which can absorb the energy from sunlight to drive electrochemical hydrogen production from the splitting of water. The substantial complexity in the scientific understanding and experimental protocols needed to sufficiently pursue accurate and reliable materials development means that a large need exists to consolidate and standardize the most common methods utilized by researchers in this field.

Table of Contents

Front Cover.
Half Title Page.
Title Page.
Copyright Page.
1: Introduction.
2: Efficiency Definitions in the Field of PEC.
3: Experimental Considerations.
4: PEC Characterization Flowchart.
5: UV-Vis Spectroscopy.
6: Flat-Band Potential Techniques.
7: Incident Photon-to-Current Efficiency and Photocurrent Spectroscopy.
8: 2-Electrode Short Circuit and j–V.
9: Hydrogen and Oxygen Detection from Photoelectrodes.
10: Stability Testing.