eBook Comprehensive Sampling and Sample Preparation, 1st Edition

  • Janusz Pawliszyn
  • Published By:
  • ISBN-10: 0123813743
  • ISBN-13: 9780123813749
  • DDC: 543.19
  • Grade Level Range: College Freshman - College Senior
  • 3200 Pages | eBook
  • Original Copyright 2012 | Published/Released August 2013
  • This publication's content originally published in print form: 2012
  • Price:  Sign in for price

About

Overview

Contains a complete treatment of the theory and methodology of sampling in all physical phases and the theory of sample preparation for all major extraction techniques.

Table of Contents

Front Cover.
Half Title Page.
Title Page.
Copyright Page.
Editor-in-Chief.
Section Editors.
Contributors.
Preface.
Contents.
1: Sampling Theory.
2: Theoretical Approaches.
3: Quality Assurance and Quality Control.
4: Methodologies for Sample Preservation and Stabilization.
5: Assessing and Controlling Sample Contamination.
6: Sample Homogenization.
7: Emerging Techniques.
8: Sampling Strategy for Process Control.
9: Integrated Total Analysis Systems.
10: Nanomaterials.
11: Gaseous Samples.
12: Indoor Air Sampling.
13: Exposure Assessment in the Workplace.
14: Aerosols PM10 and PM2.5.
15: Passive Sampling of Atmospheric Organic Contaminants.
16: Liquid Samples.
17: Surface Microlayer.
18: Equipment for Water Sampling Including Sensors.
19: Passive Sampling of Organic Contaminants in Waters.
20: Passive Sampling for Inorganic Contaminants in Water.
21: Seawater Organic Contaminants.
22: Sampling Approaches for Trace Element Determination in Seawater.
23: Sampling of Humic and Colloidal Phases in Liquid Samples.
24: Solid Samples.
25: Sampling of Fish, Benthic Species, and Seabird Eggs in Pollution Assessment.
26: Collection and Preparation of Human Biological Specimens for Contaminant Analysis.
27: Food Safety.
28: Food Contaminanants.
29: Forensic Applications.
30: Biopsic Sampling (Cancer).
31: Legal and Forensic Sampling.
Half Title Page.
Title Page.
Copyright Page.
Editor-in-Chief.
Section Editors.
Contributors.
Preface.
Contents.
1: Extraction Techniques.
2: Theory of Extraction.
3: Headspace Analysis.
4: Liquid–Liquid Extraction: Basic Principles and Automation.
5: Soxhlet Extraction and New Developments Such as Soxtec.
6: Soxhlet Extraction Versus Accelerated Solvent Extraction.
7: Accelerated Solvent Extraction (ASE) and High-Temperature Water Extraction.
8: Fundamentals of Supercritical Fluid Extraction.
9: Microwave Extraction.
10: Solvent Microextraction.
11: Dispersive Liquid–Liquid Microextraction.
12: Ionic Liquids.
13: Sorbent Chemistry, Evolution.
14: Sorbents for Gas Sampling.
15: Principles and Practice of Solid-Phase Extraction.
16: Matrix Solid-Phase Dispersion.
17: Sol–Gel Materials in Analytical Microextraction.
18: Molecularly Imprinted Polymers.
19: Monoliths, Fundamentals for Sample Preparation.
20: Bioaffinity Sorbents.
21: Nanomaterials for Sample Preparation.
22: Solid-Phase Microextraction.
23: Membrane Extraction: General Overview and Basic Techniques.
24: Hollow Fiber Liquid-Phase Microextraction.
25: Membrane Inlets for Mass Spectrometry.
26: Microdialysis Sampling in the Brain: Analytical Approaches and Challenges.
27: Extension of Extraction Technologies (Processes).
28: Analytical Derivatization Techniques.
29: Sample Preparation Automation for GC Injection.
30: LC Automation.
31: Column-Switching Sample Preparation.
32: Fundamentals and Applications of Needle Trap Devices.
33: Validation and Regulatory Issues for Sample Preparation.
Half Title Page.
Title Page.
Copyright Page.
Editor-in-Chief.
Section Editors.
Contributors.
Preface.
Contents.
1: Introduction to Extraction Techniques and Applications: Biological/Medical.
2: General Considerations when Dealing with Biological Fluid Samples.
3: Considerations on Dealing with Tissues and Cell Samples (Include Tissue Banking).
4: Cell Separation, Perfusion from Tissue, Organelle Fractionation.
5: Tissue Preparation for Microscopy and Histology.
6: Clinical Analysis.
7: Blood Sample Collection and Handling.
8: Urine Sample Collection and Handling.
9: Clinical Immunoassays and Immunosensing.
10: Preparation and Analytical Applications of Quantum Dots.
11: Newborn Screening of Genetic Diseases.
12: Issues and Pitfalls in Biomarker Development and Clinical Relevance.
13: Genomic, Proteomic and Metabolomics Analysis.
14: DNA Damage, Repair, and Genome Instability (Including Affinity Techniques).
15: Proteolytic Digestion Methods for Shotgun Proteomics.
16: Microwave Digestion of Protein Samples for Proteomics Applications.
17: Selective Enrichment of Phosphopeptides Using Nanomaterials and Monolithic Materials for the Analysis of Protein Phosphorylation.
18: Sample Preparation for Glycoproteins.
19: Sample Preparation for Single-Molecule Enzyme Assays.
20: Sampling and Sample Preparation for LC-MS-Based Metabonomics/Metabolomics of Samples of Mammalian Origin.
21: Tissue, Serum and Saliva Sampling for Proteomic Analysis.
22: Chemical Speciation, Bioavailability, Toxicology.
23: Pre-Concentration and Sample Treatment Techniques for Trace Element Analysis.
24: Enzyme Treatment of Biological Samples for Speciation.
25: Enzyme Digestion for Speciation of Arsenic.
26: Mercury Speciation and Binding to Biomacromolecules.
27: Determination of Cadmium Species Including Complexes with Metallothionein and Phytochelatin.
28: Bioaccessibility Extractions for Contaminant Risk Assessment.
29: Recent Development in Sample Preparation Techniques for Biomedical/Biological Applications.
30: Application of SPME to Pharmacodynamics, Pharmacokinetics, and Toxicology.
31: Electrospun Nanofiber-Based Solid-Phase Microextraction Media.
32: Environmental Applications.
33: Sorbent-Phase Sample Preparation in Environmental Analysis.
34: Recent Advances in Sample Preparation for Pesticide Analysis.
35: Membrane-Based Extraction for Environmental Analysis.
36: Chemical Warfare Agents: Development and Applications of Sample Preparation Approaches.
37: Sample Pretreatment Techniques for Perfluorinated Compounds.
38: Recent Advances in Solid-Phase Microextraction for Environmental Applications.
39: Environmental Applications of Cloud-Point Extraction.
40: Sample Preparation of Complex Biological Samples in the Analysis of Trace-Level Contaminants.
41: Sample Preparation for Capillary Electrophoretic Applications.
42: Sample Preparation of Microbial Contaminants in Water.
43: Inorganic Contaminants: Sample Preparation Approaches.
44: Advances in Sample Preparation of Environmental Solid Matrices.
45: Environmental and Biological Applications of Stir Bar Sorptive Extraction.
46: Sample Preparation for Food Contaminant Analysis.
47: Liquid-Based Microextraction Techniques for Environmental Analysis.
48: Forensic Applications.
49: Sample Preparation for Chromatographic Applications in Forensic Science.
50: Recent Advances in Solid-Phase Microextraction for Forensic Applications.
51: Recent Advances in Sample Preparation for Explosives.
52: New Directions in Sample Preparation for Environmental Analysis.
53: Needle-Trap Devices for Environmental Sample Preparation.
54: Use of Unconventional Solvents for Sample Preparation in Environmental Analysis.
55: Preparative Gas Chromatography as a Sample Preparation Approach.
Half Title Page.
Title Page.
Copyright Page.
Editor-in-Chief.
Section Editors.
Contributors.
Preface.
Contents.
1: Food Constituents: Volatiles.
2: Headspace Sampling in Flavor and Fragrance Field.
3: Sampling Techniques for the Determination of Volatile Components in Grape Juice, Wine and Alcoholic Beverages.
4: Sampling and Sample Preparation Techniques for the Determination of the Volatile Components of Milk and Dairy Products.
5: Sampling Techniques for the Determination of Volatile Components in Food of Animal Origin.
6: Sampling Techniques for the Determination of the Volatile Fraction of Honey.
7: Sample Preparation for Food Flavor Analysis (Flavors/Off-Flavors).
8: In Vivo Sampling of Flavor Components.
9: Food Constituents: Non-Volatiles or Semivolatiles.
10: Extraction Techniques for the Determination of Phenolic Compounds in Food.
11: Extraction Techniques for the Determination of Carotenoids and Vitamins in Food.
12: Sample Preparation Techniques for the Determination of Fats in Food.
13: Sample Preparation for the Determination of Carbohydrates in Food and Beverages.
14: Food Additives and Contaminants.
15: Solvent-Based Extraction Techniques for the Determination of Pesticides in Food.
16: Sorbent-Based Techniques for the Determination of Pesticides in Food.
17: Sample Preparation Techniques for the Determination of Some Food Contaminants (Polycyclic Aromatic Hydrocarbons, Mineral Oils and Phthalates).
18: Sampling Techniques for the Determination of Migrants from Packaging Materials in Food.
19: Sampling Techniques for the Determination of Mycotoxins in Food Matrices.
20: Sample Preparation Techniques for the Determination of Veterinary Drugs in Food Matrices.
21: New Technologies in Food Applications.
22: Application of Supercritical Fluid Extraction in Food Processing.
23: Accelerated Methods for Sample Preparation in Food.
24: Applications of SPE-MIP in the Field of Food Analysis.
25: Application of Stir-Bar Sorptive Extraction in Food Analysis.
26: Sample Preparation for the Determination of Metals in Food Samples.
27: Membrane-Based Extraction Techniques in Food Analysis.
28: Sample Preparation for Direct MS Analysis of Food.
Index.