Higher Education

Fundamentals of Analytical Chemistry, 9th Edition

  • Douglas A. Skoog Stanford University
  • Donald M. West San Jose State University
  • F. James Holler University of Kentucky
  • Stanley R. Crouch Michigan State University
  • ISBN-10: 0495558281  |  ISBN-13: 9780495558286
  • 1072 Pages
  • Previous Editions: 2004, 1996, 1992
  • © 2014 | Published
  • College Bookstore Wholesale Price = $309.00
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About

Overview

Known for its readability and systematic, rigorous approach, this fully updated Ninth Edition of FUNDAMENTALS OF ANALYTICAL CHEMISTRY offers extensive coverage of the principles and practices of analytic chemistry and consistently shows students its applied nature. The book's award-winning authors begin each chapter with a story and photo of how analytic chemistry is applied in industry, medicine, and all the sciences. To further reinforce student learning, a wealth of dynamic photographs by renowned chemistry photographer Charlie Winters appear as chapter-openers and throughout the text. Incorporating Excel spreadsheets as a problem-solving tool, the Ninth Edition is enhanced by a chapter on Using Spreadsheets in Analytical Chemistry, updated spreadsheet summaries and problems, an "Excel Shortcut Keystrokes for the PC" insert card, and a supplement by the text authors, EXCEL® APPLICATIONS FOR ANALYTICAL CHEMISTRY, which integrates this important aspect of the study of analytical chemistry into the book's already rich pedagogy. New to this edition is OWL, an online homework and assessment tool that includes the Cengage YouBook, a fully customizable and interactive eBook, which enhances conceptual understanding through hands-on integrated multimedia interactivity. Available with InfoTrac® Student Collections http://gocengage.com/infotrac.

Features and Benefits

  • Spreadsheet exercises and problems are integrated into the examples and end-of-chapter material in appropriate chapters to enhance student learning.
  • The accompanying spreadsheet supplement, EXCEL® APPLICATIONS FOR ANALYTICAL CHEMISTRY, 2e, helps students learn spreadsheets in the context of analytical applications.
  • Thought-provoking and research-oriented "Challenge" problems at the end of each chapter based on data from the literature, current topics of interest, and information accessible on the Internet engage students with today's hot topics.
  • The art program features Microsoft® Excel® screenshots, techniques, procedures, and applications with descriptive captions that visually reinforce student understanding.
  • Exclusive photographs taken by renowned chemistry photographer Charlie Winters make it easier for students to understand key principles and processes. Each chapter begins with an application-type photograph and an accompanying relevant and interesting story.
  • Feature boxes throughout the text cover a wide range of topics, including descriptions of Breath Alcohol Analyzers, Lap-on-a-Chip Technology, Modified Electrodes, Enzymatic Determination of Urea, GC/MS, C/MS, LC/MS/MS, and Capillary Electrophoresis in DNA Sequencing.
  • Molecular models, used liberally in most chapters, stimulate interest in the beauty of molecular structures and reinforce structural concepts and descriptive chemistry presented in general chemistry and upper-level courses.
  • A wide spectrum of applications, including developments in biology, medicine, and environmental science, illustrates the exciting nature of the field and enhances the relevancy of the material.

Table of Contents

1. The Nature of Analytical Chemistry
PART I: TOOLS OF ANALYTICAL CHEMISTRY
2. Chemicals, Apparatus, and Unit Operations of Analytical Chemistry
3. Using Spreadsheets in Analytical Chemistry
4. Calculations Used in Analytical Chemistry
5. Errors in Chemical Analyses
6. Random Errors in Chemical Analysis
7. Statistical Data Treatment and Evaluation
8. Sampling, Standardization, and Calibration
PART II: CHEMICAL EQUILIBRIA
9. Aqueous Solutions and Chemical Equilibria
10. Effect of Electrolytes on Chemical Equilibria
11. Solving Equilibrium Problems for Complex Systems
PART III: CLASSICAL METHODS OF ANALYSIS
12. Gravimetric Methods of Analysis
13. Titrimetric Methods; Precipitation Titrimetry
14. Principles of Neutralization Titrations
15. Titration Curves for Complex Acid/Bases Systems
16. Applications of Neutralization Titrations
17. Complexation Reactions and Titrations
PART IV: ELECTROCHEMICAL METHODS
18. Introduction to Electrochemistry
19. Applications of Standard Electrode Potentials
20. Applications of Oxidation/Reduction Titrations
21. Potentiometry
22. Bulk Electrolysis: Electrogravimetry and Coulometry
23. Voltammetry
PART V: SPECTROCHEMICAL ANALYSIS
24. Introduction to Spectrochemical Methods
25. Instruments for Optical Spectroscopy
26. Molecular Absorption Spectroscopy
27. Molecular Fluorescence Spectroscopy
28. Atomic Spectroscopy
29. Mass Spectrometry
PART VI: KINETICS AND SEPARATIONS
30. Kinetic Methods of Analysis
31. Introduction to Analytical Separations
32. Gas Chromatography
33. High-Performance Liquid Chromatography
34. Miscellaneous Separation Methods
PART VII: PRACTICAL ASPECTS OF CHEMICAL ANALYSIS
To access the following online-only chapters, enter ISBN 978-0-495-55828-6 at www.cengagebrain.com and visit this book's companion website.
35. Analysis of Real Samples
36. Preparing Samples for Analysis
37. Decomposing and Dissolving the Sample
38. Selected Methods of Analysis

What's New

  • OWL (Online Web Learning) is available for the first time with this Ninth Edition. OWL includes parameterized Mastery homework assignments correlated to sections in the text and parameterized end-of-chapter questions. OWL encourages students to practice multiple questions of the same type with different chemicals, wording, and numbers to ensure their mastery of the underlying chemical concepts. OWL also includes the interactive customizable Cengage YouBook and an optional Solutions Manual eBook.
  • All chapters have been rewritten for Excel 2010 (or 2007).
  • A new Chapter 29 on Mass Spectrometry incorporates atomic mass spectrometry (formerly in Chapter 28) with new material on molecular mass spectrometry.
  • New end-of-chapter problems have been added.
  • All examples are now titled for easy reference.
  • New Feature Boxes appear throughout, such as Feature 14-4 on the Master Equation. Approach.
  • Chapter 17 has a new section on Precipitation Titrations.
  • In Chapter 25, the discussion on thermal IR detectors now puts more emphasis on the DTGS pyroelectric detector.
  • Part VII on Practical Aspects of Chemical Analysis is now online to make it easier for students to access the material on preparing and analyzing real samples.
  • InfoTrac® Student Collections are specialized databases expertly drawn from the Gale Academic One library. Each InfoTrac® Student Collection enhances the student learning experience in the specific course area related to the product. These specialized databases allow access to hundreds of scholarly and popular publications - all reliable sources - including journals, encyclopedias, and academic reports. Learn more and access at: http://gocengage.com/infotrac.

Learning Resource Bundles

Choose the textbook packaged with the resources that best meet your course and student needs. Contact your Learning Consultant for more information.

Bundle: Text + OWLv2 24-Months Printed Access Card

ISBN-10: 1285716434  | ISBN-13: 9781285716435

List Price = $430.95  | College Bookstore Wholesale Price = $324.00

This Bundle Includes:

  • Fundamentals of Analytical Chemistry
    List Price = $411.95  | CengageBrain Price = $411.95  | College Bookstore Wholesale Price = $309.00
  • OWLv2 24-Months Printed Access Card
    List Price = $130.00  | College Bookstore Wholesale Price = $97.50


Printed Text + OWv2 24-Months Instant Access

ISBN-10:  1305434714  | ISBN-13:  9781305434714

List Price = $430.95  | CengageBrain Price = $430.95  | College Bookstore Wholesale Price = $324.00

This Bundle Includes:

  • Fundamentals of Analytical Chemistry
    List Price = $411.95  | CengageBrain Price = $411.95  | College Bookstore Wholesale Price = $309.00
  • OWv2 24-Months Instant Access
    List Price = $130.00  | CengageBrain Price = $130.00  | College Bookstore Wholesale Price = $130.00


Printed Text + OWLv2 6-Months Instant Access

ISBN-10:  1305515714  | ISBN-13:  9781305515710

List Price = $423.95  | CengageBrain Price = $423.95  | College Bookstore Wholesale Price = $319.00

This Bundle Includes:

  • Fundamentals of Analytical Chemistry
    List Price = $411.95  | CengageBrain Price = $411.95  | College Bookstore Wholesale Price = $309.00
  • OWLv2 6-Months Instant Access
    List Price = $100.00  | CengageBrain Price = $100.00  | College Bookstore Wholesale Price = $100.00


Printed Text + OWLv2 with Student Solutions Manual 24-Months Instant Access

ISBN-10:  1305520793  | ISBN-13:  9781305520790

List Price = $490.95  | CengageBrain Price = $490.95  | College Bookstore Wholesale Price = $369.00

This Bundle Includes:

  • Fundamentals of Analytical Chemistry
    List Price = $411.95  | CengageBrain Price = $411.95  | College Bookstore Wholesale Price = $309.00
  • OWLv2 with Student Solutions Manual 24-Months Instant Access
    List Price = $181.00  | CengageBrain Price = $181.00  | College Bookstore Wholesale Price = $181.00


Printed Text + LMS Integrated for OWLv2 with MindTap Reader, 1 term (6 months) Instant Access

ISBN-10:  1337349429  | ISBN-13:  9781337349420

List Price = $423.95  | CengageBrain Price = $423.95  | College Bookstore Wholesale Price = $319.00

This Bundle Includes:

  • Fundamentals of Analytical Chemistry
    List Price = $411.95  | CengageBrain Price = $411.95  | College Bookstore Wholesale Price = $309.00
  • LMS Integrated for OWLv2 with MindTap Reader, 1 term (6 months) Instant Access
    List Price = $100.00  | CengageBrain Price = $100.00  | College Bookstore Wholesale Price = $100.00


Bundle: Text + OWLv2 with Student Solutions Manual, 4 terms (24 months) Printed Access Card

ISBN-10:  1285993039 | ISBN-13:  9781285993034

List Price = $490.95  | College Bookstore Wholesale Price = $369.00

This Bundle Includes:

  • Fundamentals of Analytical Chemistry
    List Price = $411.95  | CengageBrain Price = $411.95  | College Bookstore Wholesale Price = $309.00
  • OWLv2 with Student Solutions Manual, 4 terms (24 months) Printed Access Card
    List Price = $181.00  | College Bookstore Wholesale Price = $135.75


Efficacy and Outcomes

Reviews

"The chapters dealing with titrimetry are fairly straightforward and, in the opinion of this reviewer, one of the strengths of the text. Specifically, the majority of the problems are well-explained to the student and the problems in the back of the text are helpful, especially with the increasing difficulty of the problems as one proceeds through their completion."

— Dana Spence, Michigan State University

"The authors' do a good job of making this text both readable and engaging. I would like to think a student could sit down with a piece of paper, a calculator and pencil and work through most of these chapters in 1-2 hours with good comprehension. I enjoy the level of activity this book uses in terms of engaging you with interesting problems or real world examples."

— Lane Baker, Indiana University

Supplements

All supplements have been updated in coordination with the main title. Select the main title's "About" tab, then select "What's New" for updates specific to title's edition.

For more information about these supplements, or to obtain them, contact your Learning Consultant.

Instructor Supplements

Online Instructor's Resource  (ISBN-10: 0495558389 | ISBN-13: 9780495558385)

Available online at the Instructor's Resource Web Site (http://www.cengage.com/login), this password-protected resource contains detailed solutions to all problems from the text.

Student Solutions Manual  (ISBN-10: 0495558346 | ISBN-13: 9780495558347)

The solutions manual contains worked-out solutions for all the starred problems in the text. For added value and convenience, the Student Solutions Manual can be packaged with the text. Contact your local sales representative for more information.

List Price = $97.95  | CengageBrain Price = $97.95  | College Bookstore Wholesale Price = $73.50

Student Solutions Manual Instant Access  (ISBN-10: 1285185773 | ISBN-13: 9781285185774)

List Price = $52.00  | CengageBrain Price = $52.00  | College Bookstore Wholesale Price = $52.00

LMS Integrated for OWLv2 with MindTap Reader, 1 term (6 months) Instant Access  (ISBN-10: 1305500253 | ISBN-13: 9781305500259)

MindLinks is a new service provided by Cengage to allow for deeper integration of Cengage’s digital suite, including the OWLv2 product, into an institution’s Learning Management System (LMS). The service works by using portable links that allow two-way communication between a Learning Management System and a Cengage digital product. Cengage developed MindLinks to work with all major Learning Management Systems to expand functionality. For more information on MindLinks, contact mindlinks@cengage.com.

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LMS Integrated for OWLv2 with MindTap Reader, 4 terms (24 months) Instant Access  (ISBN-10: 1305500261 | ISBN-13: 9781305500266)

MindLinks is a new service provided by Cengage to allow for deeper integration of Cengage’s digital suite, including the OWLv2 product, into an institution’s Learning Management System (LMS). The service works by using portable links that allow two-way communication between a Learning Management System and a Cengage digital product. Cengage developed MindLinks to work with all major Learning Management Systems to expand functionality. For more information on MindLinks, contact mindlinks@cengage.com.

List Price = $130.00  | CengageBrain Price = $130.00  | College Bookstore Wholesale Price = $130.00

Student Supplements

Student Solutions Manual  (ISBN-10: 0495558346 | ISBN-13: 9780495558347)

Master problem-solving using this manual's worked-out solutions for all the starred problems in the text.

List Price = $97.95  | CengageBrain Price = $97.95  | College Bookstore Wholesale Price = $73.50

OWLv2 6-Months Instant Access  (ISBN-10: 1285185765 | ISBN-13: 9781285185767)

OWL (Online Web Learning) for FUNDAMENTALS OF ANALYTICAL CHEMISTRY, 9th Edition, contains step-by-step tutorials, interactive simulations, and homework questions with instant question-specific feedback to help you every step of the way as you master tough chemistry concepts and skills. OWL encourages you to learn at your own pace, ensuring that you’ve mastered each concept before you move on. OWL includes an iPad-compatible digital textbook, enhanced with rich multimedia learning tools and available 24/7 in OWL.

List Price = $100.00  | CengageBrain Price = $100.00  | College Bookstore Wholesale Price = $100.00

OWLv2 6-Months Printed Access Card  (ISBN-10: 1285763130 | ISBN-13: 9781285763132)

Your ticket to better chemistry grades OWLv2 is a proven system to help you succeed. Its Mastery Learning approach allows you to practice at your own pace, receive meaningful feedback and use learning resources to help you achieve better grades. Know what’s important OWLv2 concentrates on what’s most important—understanding chemistry concepts—and its technology lets you work the way that’s best for you Discover the relevance of your lessons Interactive simulations, visualizations, and tutorials integrated smoothly into your lessons. The more you learn, the better prepared you are to solve problems and analyze information – which helps you succeed in exams and in the workplace. Master the content Problems that challenge you to think about the concepts, and a platform that lets you practice what you’ve learned. OWLv2 moves you up the levels from memorization to mastery in a supportive learning environment. Student Testimonial: “I dropped the class first semester due to poor performance on quizzes. There was no OWL offered. This semester I currently have an A and I greatly attest this to OWL.” 1st-Year Student General Chemistry I, University of Dayton CTA: Ask your instructor about OWLv2 for this course. Visit us online: www.cengage.com/OWLv2

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Student Solutions Manual Instant Access  (ISBN-10: 1285185773 | ISBN-13: 9781285185774)

Prepare for exams and succeed in your mathematics course with this comprehensive solutions manual! Featuring worked out-solutions to the problems in FUNDAMENTALS OF ANALYTICAL CHEMISTRY, 9th Edition, this manual shows you how to approach and solve problems using the same step-by-step explanations found in your textbook examples.

List Price = $52.00  | CengageBrain Price = $52.00  | College Bookstore Wholesale Price = $52.00

OWLv2 with Student Solutions Manual 24-Months Instant Access  (ISBN-10: 1285839765 | ISBN-13: 9781285839769)

OWL (Online Web Learning) for FUNDAMENTALS OF ANALYTICAL CHEMISTRY, 9th Edition, contains step-by-step tutorials, interactive simulations, and homework questions with instant question-specific feedback to help you every step of the way as you master tough chemistry concepts and skills. OWL encourages you to learn at your own pace, ensuring that you’ve mastered each concept before you move on. OWL includes an iPad-compatible digital textbook, enhanced with rich multimedia learning tools and available 24/7 in OWL.

List Price = $181.00  | CengageBrain Price = $181.00  | College Bookstore Wholesale Price = $181.00

LMS Integrated for OWLv2 with MindTap Reader, 1 term (6 months) Instant Access  (ISBN-10: 1305500253 | ISBN-13: 9781305500259)

MindLinks provide an elegant environment to complete your coursework by leveraging the power of your campus LMS to place coursework, class-administration and the gradebook all in one easily accessible spot and all through a single-sign-on environment to your LMS. Log on once, and access your LMS and Cengage resources in one place.

List Price = $100.00  | CengageBrain Price = $100.00  | College Bookstore Wholesale Price = $100.00

LMS Integrated for OWLv2 with MindTap Reader, 4 terms (24 months) Instant Access  (ISBN-10: 1305500261 | ISBN-13: 9781305500266)

MindLinks provide an elegant environment to complete your coursework by leveraging the power of your campus LMS to place coursework, class-administration and the gradebook all in one easily accessible spot and all through a single-sign-on environment to your LMS. Log on once, and access your LMS and Cengage resources in one place.

List Price = $130.00  | CengageBrain Price = $130.00  | College Bookstore Wholesale Price = $130.00

Meet the Author

Author Bio

Douglas A. Skoog

Douglas A. Skoog was a professor of chemistry at Stanford University and the lead author of several best-selling texts during his career. He earned a B.S. in chemistry from Oregon State University and his Ph.D. in analytical chemistry from the University of Illinois. Dr. Skoog was the 1999 recipient of the American Chemical Society award in analytical chemistry, sponsored by the Fisher Scientific Company. That same year, he was named a fellow of the American Association for the Advancement of Science. In 1993, he received the ACS Division of Analytical Chemistry Award for Excellence in Teaching.

Donald M. West

Donald M. West (deceased) was a Professor of Chemistry at San Jose State University.

F. James Holler

F. James Holler is professor emeritus of chemistry and recipient of the Alumni Association Great Teacher Award at the University of Kentucky. He received his Ph.D. from Michigan State University. In addition to his role as co-author of several bestselling texts, he is co-creator of the world-famous Periodic Table of Comic Books.

Stanley R. Crouch

Stanley R. Crouch is professor emeritus at Michigan State University. He received his undergraduate and M.S. degrees from Stanford University and his Ph.D. in analytical chemistry from the University of Illinois. He is the recipient of the 2001 American Chemical Society Division of Analytical Chemistry Award in Chemical Instrumentation and the 1996 ACS Division of Analytical Chemistry Award for Excellence in Teaching.